
Foodstuffs - Determination of saxitoxin-group toxins in shellfish - HPLC method using pre-column derivatization with peroxide or periodate oxidation
NORM herausgegeben am 1.9.2026
Designation standards: ČSN EN 14526
Classification mark: 560077
Catalog number: 524207
Publication date standards: 1.9.2026
The number of pages: 80
Approximate weight : 240 g (0.53 lbs)
Country: Czech technical standard
Kategorie: Technische Normen ČSN
This document specifies a method for the quantitative determination of saxitoxin (STX), decarbamoyl saxitoxin (dcSTX), neosaxitoxin (NEO), decarbamoyl neosaxitoxin (dcNEO), gonyautoxin 1 and 4(GTX1,4; sum of isomers), gonyautoxin 2 and 3 (GTX2,3; sum of isomers), gonyautoxin 5 (GTX5), gonyautoxin 6 (GTX6), decarbamoyl gonyautoxin 2 and 3 (dcGTX2,3; sum of isomers), N sulfocarbamoyl gonyautoxin 2 and 3 (C1,2; sum of isomers) and N-sulfocarbamoyl gonyautoxin 1 and 4 (C3,4; sum of isomers) in (raw) mussels, oysters, scallops and clams. Laboratory experience has shown that this document can also be applied to other marine invertebrates and processed products of those species, however, no complete interlaboratory validation study according to ISO 5725-2 has been carried out so far. The method described was validated in an interlaboratory study and was also verified in a European Union Reference Laboratory for Marine Biotoxins (EURLMB)-performance test aiming the total toxicity of the samples. Toxins which were not available in the first interlaboratory study as dcGTX2,3 and dcNEO were validated in two additional interlaboratory studies