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ASTM E415-08

Standard Test Method for Atomic Emission Vacuum Spectrometric Analysis of Carbon and Low-Alloy Steel

Automatische name übersetzung:

Standard Test Method for Atomic Emission Vacuum spektrometrische Analyse von Kohlenstoff und niedrig legiertem Stahl

NORM herausgegeben am 1.6.2008

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Informationen über die Norm:

Bezeichnung normen: ASTM E415-08
Anmerkung: UNGÜLTIG
Ausgabedatum normen: 1.6.2008
SKU: NS-46719
Zahl der Seiten: 9
Gewicht ca.: 27 g (0.06 Pfund)
Land: Amerikanische technische Norm
Kategorie: Technische Normen ASTM

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Die Annotation des Normtextes ASTM E415-08 :

Keywords:

carbon steel, low-alloy steel, optical emission, spectrometric analysis, Aluminum content--ferrous alloys, Carbon content--metals/alloys, Chromium content--metals/alloys, Columbium content--metals/alloys, Copper content--metals/alloys, Manganese content--metals/alloys, Molybdenum content--metals/alloys, Nickel content--metals/alloys, Phosphorus content--metals/alloys, Spectrochemical analysis--steel, Sulfur--metals/alloys, Tin content--steel, Vanadium content--metals/alloys, Carbon steel

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Significance and Use

This test method for the spectrometric analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use this test method will be analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.

1. Scope

1.1 This test method covers the simultaneous determination of 20 alloying and residual elements in carbon and low-alloy steels in the concentration ranges shown (Note 1).

Concentration Range, %
Element	Applicable Range, %^A	Quantitative Range, %^B

Aluminum	0 to 0.075	0.02 to 0.075
Arsenic	0 to 0.1	0.05 to 0.1
Boron	0 to 0.007	0.002 to 0.007
Calcium	0 to 0.003	0.001 to 0.003
Carbon	0 to 1.1	0.08 to 1.1
Chromium	0 to 2.25	0.02 to 2.25
Cobalt	0 to 0.18	0.008 to 0.18
Copper	0 to 0.5	0.04 to 0.5
Manganese	0 to 2.0	0.10 to 2.0
Molybdenum	0 to 0.6	0.03 to 0.6
Nickel	0 to 5.0	0.02 to 5.0
Niobium	0 to 0.085	0.02 to 0.085
Nitrogen	0 to 0.015	0.004 to 0.015
Phosphorous	0 to 0.085	0.02 to 0.085
Silicon	0 to 1.15	0.07 to 1.15
Sulfur	0 to 0.055	0.01 to 0.055
Tin	0 to 0.045	0.01 to 0.045
Titanium	0 to 0.2	0.004 to 0.2
Vanadium	0 to 0.3	0.004 to 0.3
Zirconium	0 to 0.05	0.02 to 0.05

^A Applicable range in accordance with Guide E 1763 for results reported in accordance with Practice E 1950.

^B Quantitative range in accordance with Practice E 1601.

Note 1—The concentration ranges of the elements listed have been established through cooperative testing of reference materials. Included, in addition to the original data of Test Method E 415 – 71, are data from cooperative testing of a broader range of reference materials to expand the element concentration ranges.

1.2 This test method covers analysis of specimens having a diameter adequate to overlap the bore of the spark stand opening (to effect an argon seal). The specimen thickness can vary significantly according to the design of the spectrometer stand, but a thickness between 10 mm and 38 mm has been found to be most practical.

1.3 This test method covers the routine control analysis in iron and steelmaking operations and the analysis of processed material. It is designed for chill-cast, rolled, and forged specimens. Better performance is expected when reference materials and specimens are of similar metallurgical condition and composition. However, it is not required for all applications of this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

E350-23	Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
E406-19	Standard Practice for Using Controlled Atmospheres in Atomic Emission Spectrometry
E1019-18	Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques
E29-22	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E1601-19	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
E1329-10	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM MNL 7	Manual on Presentation of Data and Control Chart Analysis ASTM Manual Series, ASTM International, 8th edition, 2010.
E135-23a	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).
E1763-06	Standard Guide for Interpretation and Use of Results from Interlaboratory Testing of Chemical Analysis Methods (Withdrawn 2015)
E1806-23	Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
E1950-17	Standard Practice for Reporting Results from Methods of Chemical Analysis (Withdrawn 2023)
E2972-15(2019)	Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
E305-21	Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves

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